{"id":5977,"date":"2020-02-22T18:23:26","date_gmt":"2020-02-22T23:23:26","guid":{"rendered":"http:\/\/easinc.org\/wordpress\/?page_id=5977"},"modified":"2021-09-14T10:36:18","modified_gmt":"2021-09-14T14:36:18","slug":"e19-headspace-gas-chromatography-fundamentals-method-development-and-method-transfer","status":"publish","type":"page","link":"https:\/\/eas.org\/2024\/e19-headspace-gas-chromatography-fundamentals-method-development-and-method-transfer\/","title":{"rendered":"E21-35:  Headspace-Gas Chromatography Fundamentals, Method Development and Method Transfer"},"content":{"rendered":"<div>\n<p align=\"center\"><span style=\"text-decoration: underline;\"><em><strong>One-Day Course<\/strong><\/em><\/span><em><strong>&nbsp;<br class=\"none\">Wednesday, November 17; 8:30am &#8211; 5:00pm<\/strong><\/em><em><br><\/em><\/p>\n<\/div>\n<p align=\"center\">Dr. Matthew S Klee, XO Associates LLC, Northborough, MA<\/p>\n<p style=\"text-align: justify;\" align=\"center\"><b><span style=\"text-decoration: underline;\">COURSE DESCRIPTION<\/span><br><\/b>This course is aimed at providing a working knowledge of how gas chromatography (GC) headspace samplers work, the differences between the various headspace samplers in common use, how method setpoint parameters affect performance, repeatability, and reproducibility.<\/p>\n<p style=\"text-align: justify;\" align=\"center\"><b><span style=\"text-decoration: underline;\">WHO SHOULD ATTEND<\/span><br><\/b>This course is oriented to current headspace-GC users as well as lab supervisors responsible to ensure established methods are properly implemented. Fundamental physical and mechanical processes will be presented in a way that will help users be more comfortable and effective in operating and maintaining their instruments and in transferring legacy methods on newer instrumentation.<\/p>\n<p style=\"text-align: left;\" align=\"center\"><b><span style=\"text-decoration: underline;\">TOPICS<\/span><br><\/b><\/p>\n<ol>\n<li>Principles of Headspace Sampling<\/li>\n<li>General Headspace Designs<br>a. Pressure balanced<br>b. Valve\/loop<\/li>\n<li>Interfacing Approaches and the Impact on Performance<\/li>\n<li>General Method Parameters and how they Impact Results<br>a. Temperature<br>b. Pressure<br>c. Timing<\/li>\n<li>Changes in HS Designs Over Time and how the Changes can Affect Results<br>a. Automation<br>b. Inertness<br>c. Loop pressure control<\/li>\n<li>Best Practices that Maximize Ruggedness and Repeatability<\/li>\n<li>Method Transfer between Different Instruments<br>a. Dealing with differences<\/li>\n<\/ol>\n\n\n<div class=\"wp-block-image\"><figure class=\"alignleft size-large is-resized\"><img loading=\"lazy\" decoding=\"async\" src=\"https:\/\/eas.org\/2024\/wp-content\/uploads\/2021\/04\/Klee_Matthew.jpg\" alt=\"\" class=\"wp-image-7798\" width=\"196\" height=\"180\" srcset=\"https:\/\/eas.org\/2024\/wp-content\/uploads\/2021\/04\/Klee_Matthew.jpg 511w, https:\/\/eas.org\/2024\/wp-content\/uploads\/2021\/04\/Klee_Matthew-300x275.jpg 300w\" sizes=\"(max-width: 196px) 100vw, 196px\" \/><\/figure><\/div>\n\n\n\n<p><strong>ABOUT THE INSTRUCTOR<br>Dr. Matthew S. Klee<\/strong>, PhD, is an internationally recognized analytical instrumentation expert, scientist, inventor, and author. He is considered one of the leading authorities in the areas of GC and GC-MS instrumental analysis. In addition, Dr. Klee is renowned for the quality and relevance of his live, on-line, and on-demand technical courses and presentations and has been a regular presenter of GC and GC-MS related short courses at PittCon.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>One-Day Course&nbsp;Wednesday, November 17; 8:30am &#8211; 5:00pm Dr. Matthew S Klee, XO Associates LLC, Northborough, MA COURSE DESCRIPTIONThis course is aimed at providing [&hellip;]<\/p>\n","protected":false},"author":2,"featured_media":0,"parent":0,"menu_order":0,"comment_status":"closed","ping_status":"closed","template":"","meta":{"footnotes":"","_links_to":"","_links_to_target":""},"class_list":["post-5977","page","type-page","status-publish","hentry"],"_links":{"self":[{"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/pages\/5977"}],"collection":[{"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/pages"}],"about":[{"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/types\/page"}],"author":[{"embeddable":true,"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/comments?post=5977"}],"version-history":[{"count":9,"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/pages\/5977\/revisions"}],"predecessor-version":[{"id":8087,"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/pages\/5977\/revisions\/8087"}],"wp:attachment":[{"href":"https:\/\/eas.org\/2024\/wp-json\/wp\/v2\/media?parent=5977"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}